PDF《气相色谱 -串联质谱技术分析烟草中的 132 种农药残留》

1 Multi-reaction monitoring (MRM) parameters of the

132 pesticides and internal standard in GC-MS/ MS method No. Pesticide tR / min Parent/ product ions (m/ z) CE/ eV No. Pesticide tR / min Parent/ product ions (m/ z) CE/ eV

1 dimefox 5.

12 154.

07 / 58. 03?

10 27 diazinon 15.

22 304.

1 / 179. 06?

15 (甲氟磷) 154.

07 / 111.

05 15 (二嗪磷) 179.

06 / 137.

05 15

2 methomyl 5.

32 104.

85 / 87. 9?

5 28 monocrotophos 15.

27 192.

05 / 127. 03?

10 (灭多威) 104.

85 / 58.

03 12 (久效磷) 192.

05 / 164.

04 7

3 DBCP 5.

62 157.

00 / 75. 01?

8 29 clomazone 15.

49 125.

04 / 89. 03?

18 (二溴氯丙烷) 157.

00 / 76.

97 8 (异恶草酮) 203.

96 / 106.

99 15

4 dichlorvos 6.

86 184.

95 / 92. 98?

12 30 dicloran 15.

72 205.

97 / 175. 97?

10 (敌敌畏) 184.

95 / 108.

97 15 (氯硝胺) 207.

96 / 177.

97 10

5 disulf........