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1 H), 7.98-8.00 (m,

2 H), 7.84 (s,

1 H), 7.73-7.77 (m,

1 H), 7.61-7.64 (m,

1 H), 7.48-7.50 (d,

1 H, J = 7.2 Hz), 7.21-7.22 (t,

1 H, J = 2.4 Hz), 6.85 (d,

1 H, J = 1.2 Hz). MS (EI): m/z (%):

194 (14) [M+ +1],

193 (100) [M+ ],

192 (46) [M+ -1],

165 (31),

96 (11). Supplementary Material (ESI) for Green Chemistry This journal is ? The Royal Society of Chemistry

2008 S14

11、 S 2-phenylthiophene [T2-11, 825-55-8, Ref. 5]

1 H NMR (400 MHz, CDCl3, TMS) δ 7.58-7.60 (d,

2 H, J = 7.2 Hz), 7.33-7.36 (m,

2 H), 7.23-7.29 (m,

3 H), 7.03-7.05 (m,

1 H). MS (EI): m/z (%):

161 (11) [M+ +1],

160 (100) [M+ ],

115 (26). Supplementary Material (ESI) for Green Chemistry This journal is ? The Royal Society of Chemistry

2008 S15

12、 S 3-phenylthiophene [T2-12, 2404-87-7, Ref. 5]

1 H NMR (400 MHz, CDCl3, TMS) δ 7.61-7.63 (d,

2 H, J = 7.8 Hz), 7.42-7.47 (m,

1 H), 7.38-7.41 (m,

4 H), 7.29-7.35 (m,

1 H). MS (EI): m/z (%):

161 (13) [M+ +1],

160 (100) [M+ ],

115 (33). Supplementary Material (ESI) for Green Chemistry This journal is ? The Royal Society of Chemistry

2008 S16

13、 1-phenylnaphthalene [T2-13, 605-02-7, Ref. 5]

1 H NMR (400 MHz, CDCl3, TMS) δ 7.94-7.96 (d,

2 H,J = 9.2 Hz), 7.89-7.91 (d,

1 H, J = 8.4 Hz), 7.51-7.59 (m,

6 H), 7.45-7.49 (m,

3 H). MS (EI): m/z (%):

204 (100) [M+ ],

203 (97),

101 (21). Supplementary Material (ESI) for Green Chemistry This journal is ? The Royal Society of Chemistry

2008 S17

14、 2-phenylnaphthalene [T2-14, 612-94-2, Ref. 10]

1 H NMR (400 MHz, CDCl3, TMS) δ 8.09 (s,

1 H), 7.90-7.97 (m,

3 H), 7.76-7.81 (m,

3 H), 7.51-7.56 (m,

4 H), 7.40-7.44 (m,

1 H). MS (EI): m/z (%):

204 (100) [M+ ],

101 (11). Supplementary Material (ESI) for Green Chemistry This journal is ? The Royal Society of Chemistry

2008 S18

15、 (E)-1,2-diphenylethene [T2-15, 103-30-0, Ref. 11]

1 H NMR (400MHz, CDCl3, TMS) δ 7.52-7.54 (m,

4 H), 7.35-7.39 (t,

4 H, J = 8.0 Hz), 7.25-7.29 (m,

2 H), 7.13 (s,

2 H). MS (EI): m/z (%):

180 (100) [M+ ],

165 (57),

152 (25),

102 (11),

89 (23). Supplementary Material (ESI) for Green Chemistry This journal is ? The Royal Society of Chemistry

2008 S19

16、 N O 3-(4-methoxyphenyl)pyridine [T3-1, 5958-02-1 , Ref. 12, 13]

1 H NMR (400 MHz, CDCl3, TMS) δ 8.80 (s,

1 H), 8.52-8.54 (d,

1 H, J = 4.4 Hz), 7.80-7.82 (d,

1 H, J = 7.6 Hz), 7.50-7.52 (d,

2 H, J = 8.8 Hz), 7.32 (dd,

1 H, J = 8.0, 4.8 Hz), 6.99-7.01 (d,

2 H, J = 5.2 Hz), 3.85 (s,

3 H). MS (EI): m/z (%):186 (16) [M+ +1],

185 (100) [M+ ],

170 (50),

142 (37),

115 (16),

89 (7),

63 (5). Supplementary Material (ESI) for Green Chemistry This journal is ? The Royal Society of Chemistry

2008 S20

17、 N 3-(4-Methyl-phenyl)-pyridine [T3-2, 1008-88-4, Ref. 13]

1 H NMR (400 MHz, CDCl3, TMS) δ 8.85 (d,

1 H), 8.58 (dd,

1 H, J = 4.8, 1.6 Hz), 7.85-7.88 (m,

1 H), 7.48-7.50 (m,

2 H), 7.33-7.36 (m,

1 H), 7.29-7.31 (d,

2 H, J = 8.0 Hz), 2.42 (s,

3 H). MS (EI): m/z (%):

169 (100) [M+ ],

154 (22),

153 (15),

76 (9). Supplementary Material (ESI) for Green Chemistry This journal is ? The Royal Society of Chemistry

2008 S21

18、 N 3-m-tolylpyridine [T3-3, 4385-67-5, Ref. 14]

1 H NMR (400 MHz, CDCl3, TMS) δ 8.84 (s,

1 H), 8.57-8.58 (t,

1 H, J = 2.4 Hz), 7.82 (d........