PDF《检测报告》

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7 检测报告Test Report 报告编号(Report No.): SBW20110347 1. RoHS Directive (2002/95/EC) 2. 卤素 (Halogen) 根据EN14582-2007方法处理样品,用离子色谱仪测定 As per EN14582-2007, determined by ion chromatograph 卤素(氟、氯、溴、碘)含量 Halogen ( F, Cl, Br, I ) content MDL 50mg/kg 5mg/kg Polybrominated Diphenyl Ethers ( PBDEs ) As per IEC 62321:2008, determined by gas chromatographic- mass spectrometer 检 测方法 方法检测限 1mg/kg 5mg/kg Polybrominated Biphenyls ( PBBs ) As per IEC 62321:2008, determined by gas chromatographic- mass spectrometer 多溴联苯 根据IEC 62321:2008方法,用气相色谱质谱联用仪测定 2mg/kg Lead ( Pb ) As per IEC 62321:2008, determined by inductively coupled plasma atomic emission spectrometer or atomic absorption 汞 根据IEC 62321:2008方法,用电感耦合等离子体原子发射 光谱仪进行测定 2mg/kg Mercury ( Hg ) As per IEC 62321:2008, determined by inductively coupled plasma atomic emission spectrometer As per IEC 62321:2008, determined by inductively coupled plasma atomic emission spectrometer or atomic absorption Test Item 检测项目 铅 根据IEC 62321:2008方法,用电感耦合等离子体原子发射 光谱仪或原子吸收光谱仪进行测定 六价铬 根据IEC 62321:2008方法,用紫外-可见光分光光度计测定 多溴联苯醚 根据IEC 62321:2008方法,用气相色谱质谱联用仪测定 Test Method Chromium (VI) ( Cr6+ ) As per IEC 62321:2008, determined by UV-visible spectrophotometer 检测方法 ( Test Method ) 镉 根据IEC 62321:2008方法,用电感耦合等离子体原子发射 光谱仪或原子吸收光谱仪进行测定 2mg/kg 检测项目检测方法方法检测限 Test Item Test Method MDL Cadmium ( Cd ) page

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7 检测报告Test Report 报告编号(Report No.): SBW20110347 3. PFOS 1. RoHS Directive (2002/95/EC) a. 镉、铅、汞 测试(Test for Cd / Pb /Hg contents) b. 六价铬 测试(Test for Cr6+ content) Test Item Method MDL 全氟辛烷磺酰基化合物 Perfluorooctane sulphonates (PFOS) 根据内部方法处理样品,采用液相色谱质谱 联用仪进行测定 As per in-house method for sample treatment and determined by Liquid Chromatography - Mass Spectrometry 检测项目 检测方法 方法检测限

5 mg/kg 检测流程图 ( Measurement Flowchart ) 称好样品,放进微波消解管中 Weighted sample was put into a microwave digestion vessel 加入消解试剂 Add digestion reagent 将样品在微波消解炉进行消解 Digest the sample in microwave digestion oven 消解液转移到容量瓶中 The digested solution was transferred into a volumetric flask 用去离子水定容 Made up with deionized water 用电感耦合等离子体原子发射光 谱仪或原子吸收光谱仪进行测定 Determined by ICP-AES or AAS 称好样品,将样品放入锥形瓶中 Weighted sample was put into a conical flask 加入消解液,然后将锥形瓶放在 恒温水浴摇床里加热 Add digestion solution and heat in constant temperature shaking water baths 调整抽提液pH值到 7.5 ± 0.5,转移 到比色管中,加入去离子水定容 Adjust the pH of extracted solution to 7.5 ± 0.5 and transfer into a volumetric flask,made up with deionized water 加入二苯卡巴肼溶液 Add Diphenylcarbazide solution 调整pH值到2.0±0.5,加入去离子 水定容 Adjust the pH to 2.0 ± 0.5 and make up with deionized water 用紫外可见光分光光度计进行测 定Determined by UV-visible pectrophotometer page

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7 检测报告Test Report 报告编号(Report No.): SBW20110347 c. 多溴联苯、多溴联苯醚 测试(Test for PBBs/PBDEs contents) 2. 卤素 (Halogen) 3. PFOS 称好样品,放入索氏抽提管 Weighted sample was put into a thimble 使用溶剂对样品进行索氏萃取 Extracted by solvent in Soxhlet extractor 浓缩萃取液 Concentrate the extract 转移到容量瓶中 Transfer the extract into a volumetric flask 用有机溶剂定容 Made up with organic solvent 用气相色谱质谱联用仪测定 Determined by gas chromatographic-mass spectrometer 是Yes 否No 取样、磨粉或切碎 Sampling / grinding or cutting 将吸收液倒入燃烧瓶内并将样品 秤重放入 Add absorbent in a combustion flask & place weighed sample in 将燃烧瓶充入氧气 Fill the combustion flask with oxygen 点火,燃烧完全后静置至室温 Ignite, then leave the flask at room temperature 是否有残渣残留? Any test specimen in the combustion flask? 将吸收液移入定量瓶 Transfer the absorbent into a volumetric flask 以去离子水定量 Make up with deionized water 以离子层析仪分析 Analyzed by ion chromatography 称好样品,放入索氏抽提管 Weighted sample was put into a thimble 使用溶剂对样品进行索氏萃取 Extracted by solvent in Soxhlet extractor 浓缩萃取液 Concentrate the extract 转移到容量瓶中 Transfer the extract into a volumetric flask 用有机溶剂定容 Made up with organic solvent 用液相色谱质谱联用仪进行测定 Determined by Liquid Chromatography - Mass Spectrometry page